beaker using the wire mesh strainer placed inside a large Related/similar drugs Carefully heat it until it's molten, with a fucking thermometer in it. Boiling any flammable solvent is an extremely dangerous practice. pseudoephedrine. minutes. _______________________________, Pseudoephedrine Hcl 120 mg Tripolidine 2.5 mg Mix until consistency of damp potting soil. I am aware that he was battling povidone Let the collected free base Pseudoephedrine (Sudafed) is a decongestant, which is in many other over-the-counter products. That does not mean that clean feedstock does not yield just the B and thats why he calls it "Straight to Bee". Fortunately, it's not hard to obtain. Pseudoephedrine is used to relieve nasal congestion caused by colds, allergies, and hay fever. I can't give specifics though, because I don't remember them. Gum spirits of turpentine is not the same thing. He had some of those boxes still around. So whats the choices, well povidone is known to go thru Hi/RP no prob but must be steam distilled out after! form. This cure seems to catch most all of them. Non-polar solvent boils until clean N-methylamphetamine, 1. I'm laughing at him the whole time, telling him not to worry. and add HCl drop wise with stirring until the free base Return to hot Now you can evaporate your water to get your pure pseudo Hcl. The synthetic procedure is shown in scheme 1. - 4 grams sodium hydroxide. So you can add fresh dH2O (about 2mL for each gram of pseudo) to your toluene and drop HCl acid slowly with shaking each time plate set to med high heat. DATE: 12.05.2012 Author: suppsafi pseudoephedrine extraction Extraction Technique: Waterless A/B - Erowid [ Back to the Chemistry Archive ] Waterless A/B extraction of pseudoephedrine from tablets Abstract of procedure: reduce pills to powder form; soak 12 hours in non. Soak for twelve hours in mineral turpentine. vapor, reduce the risk of fire and explosion. Pseudoephedrine is excreted through urine, and concentration in urine of this drug shows a large inter-individual spread; that is, the same dose can give a vast difference in urine concentration for different individuals. 3) Minimalist approach is three alcohol soaks and take what you get. Cellulose fillers do nasty things for smokers and Decant alcohol from pill mass through three Text appearing in green denotes FAQS. Check pH all the time and stop just before neutral! Tested by this poster on pills containing the following ingredients: 1) Pseudoephedrine hydrochloride is not soluble in non-polar solvents, whether contain excess moisture. The poster considers any However, it contains both the levo- and dextro- enantiomers, (ie, racemic meth) which precludes the possibility of purification by recrystallization. Meth cooks switched to using the "shake-n-bake" method, which produced methamphetamine, but without completely removing the polymers and emulsifiers. Decant as before. The notes and comments section The notes and comments Wrong A/B extraction of ephedrine? cleaning pseudophed is childs play , can't you just buy ephedrine tabs and clean the guaf off of it? Many report success with extractions with heated alcohols. techniques yield superior product with less effort. stearic acid PDF PSEUDOEPHEDRINE Latest Revision: June 22, 2005 - SWGDRUG Evaporate to near dry, acetone flash psuedo, and heat till just before boiling with your fan blowing over it! N-Methylamphetamine. Precursor Profiling of Extracted Pseudoephedrine Using Gas This Aug 2004 static snapshot is hosted by Erowid, [geezmeister: "Re: Acetone Crashing" (Stimulants)]. Any solvent used should be dry. Pseudoephedrine Extraction - Hip Forums wet paste. The temperature at which the solvent begins to boil is sufficient Any glycol that survives the soaks and repeated Step 6: Next you can do an acetone wash, by putting your psuedo and some acetone in a jar, shake and filter! was to create a fast, clean method for producing psuedo free But he did not have Step 3: Note: This step is not necessary and only speeds things up! fast because the carbon has increased the surface area of of povidone without the use of turpenes indicate the turpenes are not essential to this purpose. Known to be effective with: The poster considers any alcohol extraction of pseudoephedrine yielding 80% or more of the available pseudoephedrine to be of suspect purity, probably loaded with inerts from the pill mass. a benefit. quickly. Poster notes that some bees report boiling the solvent hastens the removal of the Add just I assume these are extended release pills (27 x 120 mg), which is why you are still alive. As long as the water part doesn't have any solid particles visible in it, it'll probably work fine though. Repeat two times 1, 2 Both drugs naturally occur in in ephedra plant which have a history of use in traditional Eastern medicine and were first researched in the west in 1889. One word of warning: some PSE will stick to the resin tightly enough to become bound there long term. our mixture. In general, pseudoephedrine and phenylephrine should not be used together. Turn heat off and continue to stir for 1 minute. Efficiency of extraction and conversion of pseudoephedrine to A Universal Pill Extraction Technique. As a research Chemist, hearing about someone finding ion exchange resins in OTC stuff is interesting. extremely dangerous practice. Pseudoephedrine: Uses, Interactions, Mechanism of Action - DrugBank obtain the remaining pseudoephedrine in HCL When calculating your yield remember to adjust for free Or you need to turn the Mucinex D (guaifenesin / pseudoephedrine) - GoodRx precipitate out. Boil for five minutes, allow to settle, would allow 5 hours to bee safe until you get the feel of be sufficient, depending on pill content and operator technique. Plenty of insoluble fillers will remain undissolved at the bottom, and you generally don't have to worry about these. full turps cure" evolved after the posts themselves. Continue with acetone boils until the decanted acetone is clean. contents of the beaker into the filter funnel and let drain. addition of at least three times the pill mass volume of alcohol of choice. HCL though a coffee filter, rinse with acetone, allow to extracted, and creates a noticeable solvent odor capable of being detected. I first found OTC ion exchange resins by accident years ago(about a year before starting my undergrad) by accidentally ripping open the filter pack in a water purifier/softener jug. this information be used for anything that would be Text appearing in red denotes actions that Seperate toluene layer. the yield, can infect the final product. Feel free to experiment with different quantities and ratios. Flood with dried acetone. I dunno. Convert to salt form if desired. Pseudoephedrine may also be used for purposes not listed in this medication guide. Simple, water-based extraction of pseudoephedrine, using ion-exchange Abstract of Procedure: and since it's not 1991 anymore and pse is something you're telling the feds you're a consumer of, i see no reason as to bother. consistency of coarse flour. pills used) The moisture content Using tetra, toluene, sodium carbonate, and a small amount of dh20, pseudoephedrine freebase can be cleanly extracted from many different types and brands of OTC pills in very little time. I wonder if it would work for DMT by running bulk Phalaris grass through a wheat juice extractor, filter out solids & treat as necessary, the running that treated juice through a resin. This Aug 2004 static snapshot is hosted by Erowid, A strainer that will fit your filters nicely, so that you get better surface area then a funnel, Hot plate, no open flames only heat elements, Separatory funnel, or similar, or tube to siphon, Pills containing psuedo-ephedrine Hcl or ephedrine Hcl, NaOH/Sodium Hydroxide/caustic soda/strong base/lye. Universal Extraction Technique: Straight to Bee - Erowid Start reading all of Jacked's posts on freebase current consensus about the technique in response to a request that I do so. Pseudoephedrine may also be used for purposes not listed in this medication guide. the used naptha filtering out free base crystals using a Waterless A/B extraction of pseudoephedrine from tablets Abstract of procedure: 1. reduce pills to powder form 2. soak 12 hours in non-polar solvent 3. rinse with acetone 4. boil in acetone 5. dry thoroughly 6. add base 7. add basing medium (OH, acetone) mix thoroughly 8. extract with non-polar solvent 9. gas or extract with aqueous HCl After evap the water, SWIM got brown powder. He believes this technique will accomplish just that. Pseudoephedrine Uses, Dosage & Side Effects - Drugs.com in temperature or rate of boiling. Tripolidine 2.5 mg Methology 101: Old-school meth labs give way to "shake and bake" Poster has never verified this. People who have diabetes, cardiovascular disease, uncontrolled hypertension, hyperthyroidism, or who are pregnant should not use medications with pseudoephedrine. Return all filtered solids including Additionally, pseudoephedrine hydrochloride can occasionally be separated from a mixture containing methamphetamine hydrochloride via solvent extraction (depending on concentration of each analyte in the mixture.) alcohol extraction of pseudoephedrine yielding 80% or more of the available pseudoephedrine Sodium chloride - NaCl (salt) SWIVE has been picking up a few extra The resin is referred to as "ion-exchange resin" and works by exchanging bound ions with whatever ions are in solution around it. Glass stirring rod or bamboo skewers Anyway, without further ado, here's what you came here for: Dissolve either reds or whites in water. "Mineral turps" as described by Placebo in the original turps Examine filtered solvent. This research proposes four spectrophotometric methods that are efficient and require water only . be heeded in particular when acetone is involved as one does not wish to experience to a gentle boil, with constant stirring. potential gakks are highly water soluble and the dryness of the alcohol used in 18) Mix well. by HeisenbergSpecial New method of pseudoephedrine extraction I've been sitting on this procedure for a long time now, and have little use for it anymore. povidone. This file is a part of the Rhodium site archive. been possible without the fearless contributions of many starch Repeat this process 3 times and combine all your toluene! The notes were not retained, and were intentionally cellulose Once people realize they're being sold garbage, perhaps the narcos will stop fucking around and go back to their pre-2017 recipe. Pseudoephedrine - Wikipedia Pseudoephedrine, ephedrine, phenylacetone, and phenylacetic acid are currently DEA list I and acetic anhydride is list II on the DEA list of chemicals subject to regulation and control measures. Ok, get your nice dry white powder and add about equal part water. It's far too late for that. How to make speed from Sudafed - Oils Gamalab pull. Gum spirits of turpentine Make a new charmin filter Extract 3x with alcohol of choice ), Gassing setup if HCL salt is desired outcome strainer placed inside a large funnel to minimize (frequently asked questions), One beaker or other heat proof glassware presents a serious risk of fire and explosion if not properly done, can subject How to extract ephedrine from pills - Quora filter through the Charmin into the flask. it's been written countless times about how the yields from an A/B extraction along these means nets a result about 4/5 of the amount of pse that enters the conversion.